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National Repository of Grey Literature

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Optimization of experimental conditions for measurements of perfluorinated organic acids by GC Ston, Martin ; Čabala, Radomír (advisor) ; Coufal, Pavel (referee) Commercial software Pro ezGC was used for calculation of optimal temperature program for analysis of isobutylesters of perfluorinated organic acids (C6 - C12) by gas chromatography with flame ionization detector. Optimization was done with respect to the complete resolution of all peaks of analytes. The calculated temperature program was also applied to the analysis of substances of interest on GC-MS. The calculated and measured values have been compared. The measured resolutions were higher than the calculated ones in all cases. Keywords: perfluorinated organic acids, isobutylesters, peak resolution Subject words: gas chromatography, numerical optimization Detailed record

Optimization of experimental conditions for measurements of perfluorinated organic acids by GC Ston, Martin ; Coufal, Pavel (referee) ; Čabala, Radomír (advisor) Commercial software Pro ezGC was used for calculation of optimal temperature program for analysis of isobutylesters of perfluorinated organic acids (C6 - C12) by gas chromatography with flame ionization detector. Optimization was done with respect to the complete resolution of all peaks of analytes. The calculated temperature program was also applied to the analysis of substances of interest on GC-MS. The calculated and measured values have been compared. The measured resolutions were higher than the calculated ones in all cases. Keywords: perfluorinated organic acids, isobutylesters, peak resolution Subject words: gas chromatography, numerical optimization Detailed record

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